Process for producing phenyl chlorothioformates

Details Process for producing phenyl chlorothioformates Process for producing phenyl chlorothioformates

1986-05-14

1987-09-22

Jiles, Henry R.

Organic compounds -- part of the class 532-570 series

Organic compounds

Esters having the thiocarboxylate group, -cx-, wherein the...

C07C 6800

Patent

active

046956441

ABSTRACT:
Phenyl chlorothioformates are produced in high yields easily and safely by (1) allowing sulfur dioxide to react with a mixed solution consisting of perchloromethyl mercaptan, an organic solvent and water, (2) removing the aqueous layer from the reaction mixture and (3) adding to the organic layer a phenol compound and a dehydrohalogenating agent in that order.

REFERENCES:
patent: 3165544 (1965-01-01), Tilles

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