Process for producing pentachloro-nitrobenzene

Chemistry of carbon compounds – Miscellaneous organic carbon compounds – C-metal

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C07C 7912

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041477324

ABSTRACT:
An improvement is disclosed in the preparation of pentachloronitrobenzene by the nitration of pentachlorobenzene. The improvement, which is primarily aimed at reducing the residual level of the undesirable starting material, pentachlorobenzene, in the product, includes a two-stage reactant mixing step wherein the pentachlorobenzene is first mixed with sulfuric acid and then concentrated nitric acid is added to this mixture.

REFERENCES:
patent: 3026358 (1962-03-01), Lojewski
patent: 3984487 (1976-10-01), Watts, Jr. et al.
patent: 4026955 (1977-05-01), Breaux et al.
patent: 4057950 (1977-11-01), Gay

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