Chemistry of carbon compounds – Miscellaneous organic carbon compounds – C-metal
Patent
1975-08-08
1977-01-04
Rotman, Alan L.
Chemistry of carbon compounds
Miscellaneous organic carbon compounds
C-metal
C07D21355
Patent
active
040012573
ABSTRACT:
Nicotinic acid is produced by oxidizing dialkylpyridine such as 2-methyl-5-ethylpyridine, 2,5-lutidine and the like, with nitric acid by an amount of 100 to 118 percent, preferably 100 to 108 percent, to the theoretical oxidizing amount, at a temperature of 220.degree. to 240.degree. C, preferably 225 to 235.degree. C under a pressure of 30 to 45 kg/cm.sup.2 for 5 to 30 minutes.
REFERENCES:
patent: 3657259 (1972-04-01), Stocker et al.
patent: 3741976 (1973-06-01), Stocker et al.
Kizawa Hidenori
Masuda Keiji
Otaki Yasuhiko
Nippon Soda Company Limited
Oujevolk George B.
Rotman Alan L.
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