Process for producing N-chloromethyl nitramines

Organic compounds -- part of the class 532-570 series – Organic compounds – Amino nitrogen containing

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564107, C07C24302

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active

052430758

ABSTRACT:
1-acetoxy-2,4,6-trinitro-2,4,6-triazaheptane, 1,7-diacetoxy-2,4,6-trinitro-2,4,6-triazaheptane, or 1,9-diacetoxy-2,4,6,8-tetranitro-2,4,6,8-tetraazanonane is reacted with a mixture of concentrated hydrochloric acid and trifluoroacetic 2,4,6-triazaheptane, 1,7-dichloro-2,4,6-trinitro-2,4,6-triazaheptane, or 1,7-dichloro-2,4,6,8-tetranitro-2,4,6,8-tetraazanonane.

REFERENCES:
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patent: 4203897 (1980-05-01), Kamiya et al.
patent: 5079375 (1992-01-01), Caciagli et al.
Majer et al. "Syntheses auf Dem Gabiet der Mitamise, etc." Coll. Czech Chem omm. vol. 31, 1966, p. 2547.
Solomons, Organic Chemistry 2nd Ed. John Wiley and Sons New York, pp. 768-769.

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