Process for producing N-chloromethyl nitramines

Details Process for producing N-chloromethyl nitramines Process for producing N-chloromethyl nitramines

1992-07-13

1993-09-07

Raymond, Richard L.

Organic compounds -- part of the class 532-570 series

Organic compounds

Amino nitrogen containing

564107, C07C24302

Patent

active

052430758

ABSTRACT:
1-acetoxy-2,4,6-trinitro-2,4,6-triazaheptane, 1,7-diacetoxy-2,4,6-trinitro-2,4,6-triazaheptane, or 1,9-diacetoxy-2,4,6,8-tetranitro-2,4,6,8-tetraazanonane is reacted with a mixture of concentrated hydrochloric acid and trifluoroacetic 2,4,6-triazaheptane, 1,7-dichloro-2,4,6-trinitro-2,4,6-triazaheptane, or 1,7-dichloro-2,4,6,8-tetranitro-2,4,6,8-tetraazanonane.

REFERENCES:
patent: 2856429 (1958-10-01), Sauer
patent: 4203897 (1980-05-01), Kamiya et al.
patent: 5079375 (1992-01-01), Caciagli et al.
Majer et al. "Syntheses auf Dem Gabiet der Mitamise, etc." Coll. Czech Chem omm. vol. 31, 1966, p. 2547.
Solomons, Organic Chemistry 2nd Ed. John Wiley and Sons New York, pp. 768-769.

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