Process for producing mixture containing 4-(4-methyl-4-hydroxyam

Details Process for producing mixture containing 4-(4-methyl-4-hydroxyam Process for producing mixture containing 4-(4-methyl-4-hydroxyam

1975-10-07

1977-02-08

O'Keefe, Veronica

Compositions

Electrically conductive or emissive compositions

Metal compound containing

260598, C11B 900

Patent

active

040071375

ABSTRACT:
A process is described for reacting acrolein having the structure: ##STR1## with myrcenol having the structure: ##STR2## in the presence of a Lewis acid catalyst which is one of zinc chloride, zinc bromide or stannic chloride or mixtures thereof to produce a mixture containing a major proportion of 4-(4-methyl-4-hydroxyamyl)-.DELTA..sup.3 -cyclohexenecarboxaldehyde which possesses a sweet, lilac-lily aromatic odor. The products produced by the aforementioned process are useful in various aspects of perfumery.

REFERENCES:
patent: 2842598 (1958-07-01), Kitchens
patent: 2947780 (1960-08-01), Teegarden et al.
patent: 3030384 (1962-04-01), Somerville
patent: 3067244 (1962-12-01), Robinson et al.
E. F. Lutz et al. J. Amer. Chem. Soc. 86, 3899 1964.

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