Process for producing metal halide-amide reaction product

Details Process for producing metal halide-amide reaction product Process for producing metal halide-amide reaction product

1976-09-14

1978-09-19

Sneed, Helen M. S.

Chemistry of carbon compounds

Miscellaneous organic carbon compounds

C-metal

260429R, 2604293, C07F 728

Patent

active

041154231

ABSTRACT:
A process for the preparation of a metal halide-amide reaction product, useful in the preparation of metal-modified amide-aldehyde polymers, which comprises
(1) reacting in a water-immiscible inert liquid medium a metal halide with at least one amide having at least two replaceable hydrogens to obtain a reaction product therebetween;
(2) hydrolyzing the reaction product obtained in step (1) above with water to form an aqueous solution of the reaction product;
(3) partially neutralizing the aqueous solution of the reaction product obtained in step (2) with a bicarbonate, and
(4) recovering the metal halide-amide reaction product obtained.

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