Process for producing inorganic acid salts of tertiary butyl hyd

Details Process for producing inorganic acid salts of tertiary butyl hyd Process for producing inorganic acid salts of tertiary butyl hyd

1980-06-30

1982-01-12

Doll, John

Organic compounds -- part of the class 532-570 series

Organic compounds

Amino nitrogen containing

C07C10902

Patent

active

043106960

ABSTRACT:
Inorganic acid salts of tertiary butyl hydrazine such as hydrochloride or hydrobromide of tertiary butyl hydrazine, useful for production of azine compounds are substantially stoichiometrically produced by reaction of inorganic acid salts of hydrazine such as hydrochloride or hydrobromide of hydrazine with tertiary butyl halides such as chloride or bromide at a molar ratio of the tertiary butyl halides to inorganic acid salts of 1:7-10 at a reaction temperature of 90.degree. to 110.degree. C. for 40 to 100 minutes.

REFERENCES:
patent: 2445518 (1948-07-01), Dreyfus
patent: 3005027 (1961-10-01), Druey et al.
patent: 3272807 (1966-09-01), Biel et al.
Smith, "The Chemistry of Open-Chain Organic Nitrogen Compounds", vol. II, pp. 126 & 127, (1966).

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