Process for producing hydroxy terminated nitramines

Details Process for producing hydroxy terminated nitramines Process for producing hydroxy terminated nitramines

1992-07-13

1993-10-05

Hollrah, Glennon H.

Organic compounds -- part of the class 532-570 series

Organic compounds

Amino nitrogen containing

C07C24100

Patent

active

052507300

ABSTRACT:
A process by which 1,7-dihydroxy-2,4,6-trinitro-2,4,6-triazaheptane or 1,9-dihydroxy-2,4,6,8-tetranitro-2,4,6,8-tetraazanonane is produced by hydrolyzing 1,7-diacetoxy-2,4,6-trinitro-2,4,6-triazaheptane or 1,9-diacetoxy-2,4,6,8-tetranitro-2,4,6,8-tetraazanonane with concentrated aqeuous hydrochloric acid comprising from 28 to 32 weight percent of hydrogen chloride with the remainder being water.

REFERENCES:
Reed, Jr., "Tetramethylenetrinitramine Trifluoroacetates", J. Amer. Chem. c., vol. 78, No. 4, (Feb. 20, 1956), pp. 801-804.
Solomons, Organic Chemistry, 2nd Ed., John Wiley and Sons, New York, (1980), pp. 768-771.

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