Organic compounds -- part of the class 532-570 series – Organic compounds – Carboxylic acids and salts thereof
Patent
1997-07-07
1998-07-07
Barts, Samuel
Organic compounds -- part of the class 532-570 series
Organic compounds
Carboxylic acids and salts thereof
C07C 5142
Patent
active
057771618
ABSTRACT:
There is disclosed a process for producing highly pure terephthalic acid by the use of a dispersion medium replacement apparatus equipped with a stirring unit at the bottom portion for uniform dispersion, wherein an original slurry comprising a first dispersion medium and terephthalic acid crystals is introduced into a dispersion medium replacement apparatus at the top portion, a second dispersion medium is introduced into the apparatus at the bottom portion, a replaced slurry comprising principally the second dispersion medium and the terephthalic acid crystals is taken out from the apparatus at the bottom portion, and the first dispersion medium as a major component is taken out from the apparatus at the top portion, which process comprises maintaining a uniformly dispersed slurry at the bottom portion of the apparatus at a concentration higher than that of a slurry at the intermediate portion; maintaining the upper portion at a higher temperature in a vertical temperature distribution therein to form a temperature change zone; and controlling the feed rate of the second dispersion medium and/or the takeout rate of the replaced slurry according to the location of the temperature change zone. By virtue of the specific control system, that is, taking advantage of the temperature change zone, the apparatus can be steadily operated with ease and high reliability at a high replacement efficiency, and thus highly pure terephthalic acid is stably obtained.
REFERENCES:
patent: 5679847 (1997-10-01), Ohkoshi et al.
patent: 5684187 (1997-11-01), Ohkoshi et al.
patent: 5705682 (1998-01-01), Ohkoshi et al.
Barts Samuel
Mitsubishi Gas Chemical Company Inc.
Mizushima Aroma Company, Ltd.
Toyo Boseki Kabushiki Kaisha
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