Process for producing concentrate of unsaturated fatty acid

Organic compounds -- part of the class 532-570 series – Organic compounds – Fatty compounds having an acid moiety which contains the...

Reexamination Certificate

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C554S199000, C554S206000

Reexamination Certificate

active

07439377

ABSTRACT:
An easy and inexpensive process by which a concentrate of a given unsaturated fatty acid can be obtained from a mixture which has conventionally been difficult to concentrate. The process, which is for producing a concentrate of a desired isomer (a) from a mixture (A) selected from the group consisting of a mixture comprising at least two isomers of a C16or higher conjugated unsaturated fatty acid and a mixture comprising at least two cis-isomers of a C16or higher unsaturated fatty acid having a cis-double bond, is characterized by comprising: a step in which the mixture (A) is mixed with at least one C4-14saturated fatty acid (B) to obtain a mixture solution containing the isomer (a) dissolved therein; a crystallization step in which either crystals rich in the isomer (a) or crystals poor in the isomer (a) are precipitated from the mixture solution; and a solid-liquid separation step for obtaining the crystals rich in the isomer (a) or for obtaining a solution rich in the isomer (a) by removing the crystals poor in the isomer (a).

REFERENCES:
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O. Berdeaux, et al., A simple Method of Preparation of Methyl trans 10, cis-12- and cis-9, trans-11-Octadecadienoates from Methyl Linoleate J. Am. Oil. Chem. soc., 1998, vol. 75, No. 12, pp. 1749-1755.
International Search Report for PCT/JP2005/017487 dated Sep. 22, 2005.

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