Process for producing columbite-type niobate and process for pro

Details Process for producing columbite-type niobate and process for pro Process for producing columbite-type niobate and process for pro

1993-11-10

1994-11-22

Cooper, Jack

Chemistry of inorganic compounds

Oxygen or compound thereof

Metal containing

423593, 423595, 501134, 501135, C01G 2100, C01G 3300

Patent

active

053667182

ABSTRACT:
A process for producing a columbite-type niobate and a process for producing a niobium-containing lead-type perovskite compound using the columbite-type niobate. A precursor slurry of a columbite compound composed of a fresh niobium hydroxide, a metal acetate and ammonium aqueous solution is spray-dried, and is calcined at 500.degree. C. or higher to obtain a crystalline columbite-type compound having grain sizes of 1 .mu.m or smaller to which was then mixed a lead component. The mixture is calcined, pulverized and is sintered at a temperature of 800.degree. to 1100.degree. C. to synthesize a highly dielectric material of a niobium-containing lead-type composite perovskite. The precursor of columbite is calcined at 500.degree. to 1100.degree. C. to obtain fine columbite-type niobate crystals of grain sizes of 1 .mu.m or smaller. A lead-type perovskite compound using the above crystals can be sintered at a temperature of as low as 950.degree. C. or lower, and the sintered product thereof has a homogeneous and fine texture and excellent dielectric properties that could not be obtained by the conventional solid-phase process.

REFERENCES:
patent: 5180699 (1993-01-01), Terada et al.
patent: 5229101 (1993-07-01), Watanabe et al.
patent: 5288474 (1994-02-01), Reichert et al.

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