Process for producing chlorosulfonyl isocyanate

Chemistry of inorganic compounds – Nitrogen or compound thereof – Carbon containing

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C01B 1745

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051184877

ABSTRACT:
Provided is a process for producing chlorosulfonyl isocyanate by reacting sulfur trioxide with cyanogen chloride, which comprises feeding sulfur trioxide and cyanogen chloride simultaneously to the reaction zone and maintaining the temperature of the reacting zone at 10.degree. to 50.degree. C. This is a commercially very simple process and can produce chlorosulfonyl isocyanate with high purity in high yield.

REFERENCES:
patent: 3375088 (1968-03-01), Onodera et al.
Graf, Angew. Chem. Int'l vol. 7 #3 (1968) pp. 172-173.
Organic Synthesis pp. 226-231.

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