Process for producing acicular goethite particles and acicular m

Details Process for producing acicular goethite particles and acicular m Process for producing acicular goethite particles and acicular m

1993-02-25

1995-03-21

Cooper, Jack

Compositions

Magnetic

Iron-oxygen compound containing

423632, 423633, 423634, 427127, 427128, C01G 4906, C01G 4908

Patent

active

053992784

ABSTRACT:
Disclosed herein are a process for producing acicular goethite particles comprising the steps of: blowing an oxygen-containing gas into a ferrous salt reaction solution containing colloidal ferrous hydroxide or iron-containing colloidal precipitates which is obtained by reacting an aqueous ferrous salt solution with less than one equivalent of an aqueous alkali hydroxide solution and/or an aqueous alkali carbonate solution based on Fe.sup.2 + in said aqueous ferrous salt solution so as to oxidize said colloidal ferrous hydroxide or iron-containing colloidal precipitates and to produce acicular goethite nucleus particles, adding to the resultant aqueous ferrous salt reaction solution containing said acicular goethite nucleus particles not less than one equivalent of an aqueous alkali carbonate solution based on Fe.sup.2 + in said aqueous ferrous salt reaction solution, and blowing an oxygen-containing gas into the mixed aqueous ferrous salt reaction solution so as to grow said goethite nucleus particles; and a process for producing acicular magnetic iron oxide particles by reducing the acicular goethite particles obtained in the above process to produce acicular magnetite particles, and if necessary, oxidizing the acicular magnetite particles to obtain acicular maghemite particles, and if necessary, modifying the acicular magnetite or maghemite particles with Co or Co and Fe.sup.2 +.

REFERENCES:
patent: 4033891 (1977-07-01), Matsui et al.
patent: 4108787 (1978-08-01), Masaki et al.
patent: 4136049 (1979-01-01), Horiishi et al.
patent: 4136158 (1979-01-01), Okuda et al.
patent: 4188302 (1980-02-01), Becker et al.
patent: 4495164 (1985-01-01), Okuda et al.
patent: 4873010 (1989-10-01), Takedoi

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