Process for producing a water soluble package

Details Process for producing a water soluble package Process for producing a water soluble package

2000-03-14

2001-08-28

Douyon, Lorna M. (Department: 1751)

Cleaning compositions for solid surfaces, auxiliary compositions

Cleaning compositions or processes of preparing

Liquid composition

C510S120000, C510S140000, C510S296000, C510S439000, C264S553000, C264S571000

Reexamination Certificate

active

06281183

ABSTRACT:

INTRODUCTION
The invention relates to a process for producing a thermoformed package of the type comprising the steps of placing a first sheet of formable film over a forming die having a cavity, moulding the film into the cavity thereby forming a recess in the film, placing a composition in the thus formed recess, and sealing a second sheet of film across the recess to close the package. In particular, the invention relates to such a process for producing a water-soluble package containing a detergent composition.
Detergent compositions for the machine washing of laundry are provided in many forms. Probably the most prevalent form of laundry detergent is washing powder or granules. A problem with the use of these forms of detergent is that the product needs to be dosed into the machine in such a way that the detergent is quickly and thoroughly dissolved in the wash water of the machine without coming into contact with the laundry in a solid form. In this regard many dosing devices which overcome this problem have been proposed. One such device disclosed in European Patent Nos. 0 343 070 and 0 343 069 teaches the use of a flexible fabric sock which holds the particulate detergent in the machine, the fabric of the sock being permeable to water so as to allow water enter the sock and carry the detergent out of the sock through the fabric walls in the form of an aqueous solution. More recently unit dose forms of detergent have been proposed in the form of compressed tablets of detergent powder. A problem encountered with the provision of detergent tablets is that the tablets need to be strong enough to withstand storage and transport, yet weak enough to disintegrate and dissolve quickly in the washing machine.
A further problem is the need to prevent the tablets “posting” in the porthole and between the drums of conventional washing machines. More recently these problems have been overcome by the provision of detergent tablets having specific chemical disintegrants which allow quick disintegration of the tablets in the aqueous environment of a washing machine, and by the provision of loosely fitting net bags which aid tablet disintegration and prevent “posting”. However, as many of the current detergent tablets contain bleach and other irritant substances, the problem of handling the tablets remains.
The provision of detergent compositions in water-soluble films has been known for some time. Most of the documents relating to this subject describe water soluble film envelopes formed using a vertical form-fill-seal (VFFS) route. A problem with envelopes produced using this VFFS method is that, due to the constraints of the process, the resultant envelopes have seals which incorporate defined weak points where the seals overlap at corners. This results in envelopes, which are easily corrupted as a result of impacts suffered during transport. In an attempt to overcome the problems associated with such VFFS envelopes, European Patent Application No. 0 608 910 describes thermoformed water soluble packages for pesticidal compositions of the above mentioned type, which packages include a seal which does not have any angular intersections with itself. While this specification does provide a partial solution to the problem of weak seals, the thermoforming of water-soluble films results in formed packages having many other weak points. Moreover, the packaging and transport of such packages subjects the formed packages to considerable impact forces. A further problem inherent with thermoforming processes, particularly when the thermoformed package is to contain liquid, is contamination of the seal with liquid, resulting in poor sealing of the packages.
It is an object of the invention to overcome at least some of the above problems.
STATEMENTS OF INVENTION
According to the invention, there is provided a process for producing a thermoformed package of the above-mentioned type, the process being characterised in that, once formed, the or each recess is substantially retained in its formed orientation by the application of a vacuum through the or each cavity. Ideally, the vacuum is maintained at least until completion of the sealing step. In this way, shrinkback of the formed recesses is minimised, thus preventing spillage of the composition contained in the formed recesses onto the sealing area of the film. The extent of vacuum to be applied should be sufficient to retain the formed recesses in their formed orientation without unduly deforming or otherwise damaging the film. In this regard the exact pressure to be applied is variable and depends on the film being formed, the type of composition being added to the recesses, and the temperature and humidity of the forming environment. Typically however, a vacuum of between 0.1 and 10 Bar will be used. The vacuum is preferably applied through at least one aperture in the at least one forming cavity. Ideally, the or each cavity will include a plurality of apertures through which the vacuum is applied. In one embodiment of the invention, the at least one cavity may comprise a porous material through which the vacuum may be applied.
Preferably, the or each cavity in the forming die has a curved edge, wherein at least a portion of the curved edge is formed from a resiliently deformable material. Ideally, a predominant portion, and most preferably a whole, of the curved edge is formed of a resiliently deformable material. In one embodiment of the invention, the curved edge comprises an annular gasket of resiliently deformable material, which gasket is mounted in a circumferential groove around the or each cavity. In such a case, the gasket should be dimensioned such that, when mounted in the groove, an exposed surface of the gasket should be flush with a surface of the cavity.
In a further aspect of the invention, the or each cavity is surrounded by a raised flange, wherein at least a portion, and ideally most or all, of the raised flange comprises resiliently deformable material. In such a case, the curved edge and flange are preferably integrally formed. Thus, a single gasket preferably comprises the curved edge and the flange. In one embodiment of the invention, a ratio of a width of the flange to a minor diameter of the cavity is between 1:50 and 1:10, preferably about 1:12.
The resiliently deformable material is preferably silicone rubber, however other suitable material performing the same function are envisaged.
In the thermoforming step of the process of the invention, the film is heated by a heating plate having at least one concave depression which in use overlies the at least one cavity, wherein the heating step involves the step of bringing the film into intimate contact with the or each depression. The use of a heating plate having concave depressions ensures that the film when heated thermoforms uniformly which results in a package having less weak spots.
In one embodiment of the invention, intimate contact between the film and the concave depression is achieved by exerting a vacuum between the depression and the film. In this regard the depression may include holes through which the vacuum may be pulled. Alternatively, the heating plate may comprise a porous material. When a vacuum is exerted in this manner, the vacuum should ideally comprise a pressure of up to 1 Bar, and preferably be less that 0.6 Bar. In an alternative embodiment of the invention, the film is forced into intimate contact with the concave depression by blowing air against it. Typically the pressure of the blown air will be less than 5 Bar, preferably less than 3 Bar. The heating plate preferably has a temperature in the region of 100 to 120 degrees C., and ideally is approximately 110 degrees C. Although the time the film contacts the heating plate depends to a large extent on the type of film used and the temperature of the heating plate, the time of contact between the film and the plate should be in the region 0.1 to 5 seconds, preferably 0.5 to 1 seconds, ideally approximately 700 milliseconds.
In a particularly preferred embodiment of the invention, the at leas

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