Process for producing a low viscosity silicone resin

Chemistry of carbon compounds – Miscellaneous organic carbon compounds

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260 28R, 260 37SB, 260 465G, C08G 7704

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040268683

ABSTRACT:
A process for producing a low viscosity silicone resin which comprises hydrolyzing halosilanes in a heterogeneous hydrolysis mixture of water, acetone and a water-immiscible solvent where the critical aspects of the process are the addition of the chlorosilanes to the hydrolysis medium by first mixing them with a portion of the acetone and adding them to the hydrolysis mixture over a period of at least 40 minutes and maintaining the temperature of said hydrolysis medium such that it does not exceed 45.degree. C. The silicone resins produced by this process are useful in producing molding compositions having a low coefficient of thermal expansion.

REFERENCES:
patent: 3489782 (1970-01-01), Pruvost et al.
patent: 3666830 (1972-05-01), Alekna
patent: 3792012 (1974-02-01), Zdaniewski

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