Process for producing a high purity aromatic polycarboxylic...

Organic compounds -- part of the class 532-570 series – Organic compounds – Carboxylic acids and salts thereof

Reexamination Certificate

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Reexamination Certificate

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07547803

ABSTRACT:
A process for producing a high purity aromatic polycarboxylic acid (APA) by purification of a crude APA comprises: (I) aging a slurry of the crude APA in a first dispersion medium at 180 to 300° C. for 10 minutes or longer under stirring; (II) introducing the aged slurry of the APA into a column for substituting dispersion media, bringing the slurry into contact with a second dispersion medium and separating the resultant fluid into a fluid of the first dispersion medium containing impurities and a slurry of the second dispersion medium containing crystals of the high purity APA; and (III) separating the crystals of the high purity APA from the slurry of the second dispersion medium. A high purity APA having excellent hue and particle diameter can be industrially advantageously produced while the construction of the process is simplified and the consumption of energy is decreased.

REFERENCES:
patent: 5354898 (1994-10-01), Schroeder
patent: 5362908 (1994-11-01), Schroeder et al.
patent: 5756833 (1998-05-01), Rosen et al.
patent: 2002/0002303 (2002-01-01), Rosen
patent: 07-149690 (1995-06-01), None
patent: 09-151162 (1997-06-01), None
patent: 2000-001456 (2000-01-01), None

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