Process for producing 3-hydrazino-4-amino-5-mercapto-1,2,4-triaz

Details Process for producing 3-hydrazino-4-amino-5-mercapto-1,2,4-triaz Process for producing 3-hydrazino-4-amino-5-mercapto-1,2,4-triaz

1975-07-07

1978-04-04

Rush, Raymond V.

Chemistry of carbon compounds

Miscellaneous organic carbon compounds

C-metal

260308C, C07D24912

Patent

active

040827631

ABSTRACT:
A process for the production of 3-hydrazino-4-amino-5-mercapto-1,2,4-triazole wherein hydrazinium-dithiocarbazinate is heated at moderately elevated temperature, e.g. about 50.degree. C. to 85.degree. C. and under reduced pressure, e.g. about 50 to 500 mm. Hg, with at least a 3.times. molar amount of hydrazine hydrate.

REFERENCES:
patent: 2726263 (1955-12-01), Audrieth et al.
patent: 3929877 (1975-12-01), Toth et al.
Audrieth et al., J. Org. Chem., vol. 19, pp. 733-741 (1954).

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