Process for producing 3,4-caranediol

Details Process for producing 3,4-caranediol Process for producing 3,4-caranediol

1995-09-08

1997-03-04

Sellers, Robert E.

Organic compounds -- part of the class 532-570 series

Organic compounds

Heterocyclic carbon compounds containing a hetero ring...

549512, 549513, 549523, 549525, 549531, 549545, 549546, 568807, 568817, 568822, 568823, C07D30119

Patent

active

056080883

ABSTRACT:
A process for producing 3,4-caranediol of the formula [I] includes subjecting 3,4-epoxycarane, which is obtained by epoxidizing 3-carene under specific conditions, to a hydration reaction in the presence of a base catalyst in aqueous ethanol under pressure to obtain 3,4-caranediol.

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Andrew S. Kende et al., Tetrahedron Letters, A New Paradigm for Alkene. . ., vol. 35, No. 44, Oct. 31, 1994, pp. 8123-8126.
E. KH. Kazakova et al., Chemical Abstracts, Alkali-catalyzed hydration. . ., vol. 100, No. 11, Mar. 12, 1984 CA No. 85936r.
Erkki Kolehmainen, J. Chem. Soc. Persin Trans. 2, Oxygen-containing Bicyclic. . ., No. 4, 1993 Letchworth GB, pp. 641-648.
Synthetic Communication, 19, 1939-43 (1989) Payne, et al., "Reactions of Hydrogen. . .", J. Org. Chem., vol. 26, 1961, pp. 659-663.
Eto, et al., "Epoxides", Chem. Abst., 86, 55595d, Jul. 1976.

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