Process for preparing xanthine phosphodiesterase V...

Organic compounds -- part of the class 532-570 series – Organic compounds – Chalcogen bonded directly to ring carbon of the purine ring...

Reexamination Certificate

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C544S272000, C544S271000, C544S273000, C548S326500, C560S035000

Reexamination Certificate

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07074923

ABSTRACT:
A process for preparing xanthine phosphodiesterase V inhibitors, and compounds utilized in said process. The process includes a five-step methodology for efficient synthesis of Compound 5 without intermediate purifications or separations, a dihalogenation step to synthesize Compound 7, and a coupling reaction to produce Compound 9

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