Process for preparing trialkylsilyldiazomethanes

Details Process for preparing trialkylsilyldiazomethanes Process for preparing trialkylsilyldiazomethanes

1982-07-23

1984-01-03

Shaver, Paul F.

Chemistry of carbon compounds

Miscellaneous organic carbon compounds

C-metal

260239A, C07D20100, C07F 710

Patent

active

044241585

ABSTRACT:
A process for preparing trialkylsilyldiazomethanes in which halomethyltrialkylsilane represented by the general formula R.sup.1 R.sup.2 R.sup.3 SiCH.sub.2 X (wherein R.sup.1, R.sup.2 and R.sup.3 denote an alkyl group of 1 to 4 carbon atoms, and X denotes a halogen group) is reacted with metallic magnesium to give a Grignard reagent, which is then reacted with diphenyl phosphoric acid azide.

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