Process for preparing tertiary phosphines

Details Process for preparing tertiary phosphines Process for preparing tertiary phosphines

1983-10-26

1985-03-26

Sneed, Helen M. S.

Organic compounds -- part of the class 532-570 series

Organic compounds

Phosphorus containing

568 8, C07F 950

Patent

active

045075026

ABSTRACT:
A tertiary phosphine oxide, such as triphenylphosphine oxide, is reduced to the corresponding tertiary phosphine in the presence of a sodium aluminum hydride/sodium aluminum chloride reducing agent.

REFERENCES:
patent: 3261871 (1966-07-01), Fritzsche et al.
patent: 3280195 (1966-10-01), Fritzsche et al.
patent: 3847999 (1974-11-01), Gardner et al.
patent: 4008282 (1977-02-01), Townsend et al.
patent: 4113783 (1978-09-01), Malpass et al.
patent: 4131624 (1978-12-01), Davis et al.
Chemical Abstracts 53 9879c (1959).
Chemical Abstracts 61 8335f (1964).
Chemical Abstracts 63 8398h (1966).
Kosolapoff et al., Organic Phosphorus Compounds, Wiley Intersc. Pub., N.Y., vol. 1, pp. 45-47 (1972).

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