Process for preparing solid acetyl phosphate salt

Details Process for preparing solid acetyl phosphate salt Process for preparing solid acetyl phosphate salt

1985-01-22

1988-06-28

Killos, Paul J.

Chemistry of carbon compounds

Miscellaneous organic carbon compounds

C-metal

C07F 502

Patent

active

047537574

ABSTRACT:
A salt of monoacetyl phosphate which is useful in the field of enzymatic reactions can be obtained as a precipitate by using a specified amount of lithium ion as a precipitating agent in the process for the acetylation of phosphoric acid or its salt with acetic anhydride. The resulting precipitate can be separated from the reaction mixture by filtration without necessity of operation at a low temperature or the replacement of solvents.

REFERENCES:
Avison, A. W. D., J. Chem. Soc., vol. 732, (1955), pp. 732-738.
Stadtman, E. R. et al., J. Biol. Chem., vol. 185, (1950), pp. 549-551.
Lewis, Jerome M., J. Org. Chem., vol. 44, (1979), pp. 364-365.

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