Process for preparing silicon and optionally aluminum and...

Electrolysis: processes – compositions used therein – and methods – Electrolytic synthesis – Utilizing fused bath

Reexamination Certificate

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C205S358000, C205S364000, C205S372000

Reexamination Certificate

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06974534

ABSTRACT:
Process for preparing highly purified silicon and optionally aluminum and silumin (aluminum silicon alloy) in the same cell, wherein silicate and/or quartz containing rocks are subjected to electrolysis in a salt melt containing fluoride, whereby silicon and aluminum are formed in the same bath, and aluminum formed, which may be low alloyed, flow to the bottom and is optionally drawn off, and deposit formed on the cathode is removed from the cathode and crushed, optionally together with the remaining electrolysis bath, concentrated sulfuric acid and then hydrochloric acid and water are added to the crushed material, liberated Si-grains float to the surface and are taken out and treated further as desired.

REFERENCES:
patent: 3405043 (1968-10-01), Barakat et al.
patent: 4292145 (1981-09-01), De Mattei et al.
patent: 5873993 (1999-02-01), Stubergh
patent: 9533870 (1995-12-01), None
patent: 97/27143 (1997-07-01), None

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