Process for preparing secondary amines

Organic compounds -- part of the class 532-570 series – Organic compounds – Amino nitrogen containing

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564356, 564365, C07C14924, C07C14942

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active

045408190

ABSTRACT:
New intermediates and processes for preparing 6-halo-7,8-dihydroxy-1-(p-hydroxyphenyl)-2,3,4,5-tetrahydro-1H-3-benzazepi nes involve the reaction of a p-methoxyphenylglyoxal, lower alkyl hemimercaptal with a 2-chloro-3,4-dimethoxyphenethylamine, followed by a borohydride reduction.

REFERENCES:
patent: 3345416 (1967-10-01), Russell et al.
patent: 4197297 (1980-04-01), Weinstock
H. Becker et al., J. Am. Chem. Soc., 85 3410, (1963).

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