Process for preparing phenyldichlorophosphine

Details Process for preparing phenyldichlorophosphine Process for preparing phenyldichlorophosphine

1983-12-27

1988-04-12

Moyer, Donald B.

Chemistry of carbon compounds

Miscellaneous organic carbon compounds

C-metal

C07F 952

Patent

active

047373172

ABSTRACT:
Phenyldichlorophosphine is prepared by contacting benzene with phosphorus trichloride in the vapor phase at a temperature from about 100.degree. C. to about 145.degree. C. in the presence of a catalyst consisting essentially of aluminum metal and an activating amount of aluminum chloride.

REFERENCES:
patent: 3029282 (1962-04-01), Toy et al.
patent: 3057917 (1962-10-01), Maier
patent: 3210418 (1965-10-01), Planfetti
patent: 3864394 (1975-02-01), Via et al.
patent: 3954859 (1976-05-01), Jurewicz et al.
Kosolapoff, G. M. et al., Organic Phosphorus Compounds, (1973), vol. 4, pp. 79-82, (Wiley-Interscience, Publ).
CRC Handbook of Chemistry and Physics, (1979-1980 Ed.), CRC Press, Publ., pp. B-105 and C-146.
Organic Syntheses, Coll., vol. 4, 784-785, (1963).

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