Process for preparing high 2-O-.alpha.-D-glucopyranosyl-L-ascorb

Organic compounds -- part of the class 532-570 series – Organic compounds – Carbohydrates or derivatives

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536 11, 536124, 536127, 536 41, 536 182, 536 186, 549315, C07H 106, C07H 1704, C07D30762

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active

054688507

ABSTRACT:
Disclosed is an industrial-scale preparation of a high 2-O-.alpha.-D-glucopyranosyl-L-ascorbic acid content product with an improved purity, the preparation comprising subjecting a solution containing 2-O-.alpha.-D-glucopyranosyl-L-ascorbic acid and a saccharide derivative of L-ascorbic acid exhibiting a direct reducing activity to an oxidation treatment, subjecting the resultant mixture ti column chromatography using a strongly-acidic cation exchange resin, and recoverying the resultant high 2-O-.alpha.-D-glucopyranosyl-L-ascorbic acid content fraction. Thus, the preparatiobn has a great significance in the industrial field.

REFERENCES:
patent: 3763009 (1973-10-01), Suzuki et al.
patent: 4487198 (1984-12-01), Miyake et al.
patent: 5137723 (1992-08-01), Yamamoto et al.
Nippon Eiyo Shokuryo Gakkaishi, Journal of Japanese Society of Nutrition and Food Science, vol. 43, 1990.
Science and Industry, vol. 65, 1991, pp. 265-274.
Miyake and Suzuki, "Enzymatic Formation of New L-Ascorbic Acid Glycosides.", Vitamins, vol. 43, 1971 pp. 205-209.

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