Process for preparing hexanitrobibenzyl

Details Process for preparing hexanitrobibenzyl Process for preparing hexanitrobibenzyl

1979-08-14

1981-01-13

Sebastian, Leland A.

Organic compounds -- part of the class 532-570 series

Organic compounds

Oxygen containing

C07C 7910

Patent

active

042451299

ABSTRACT:
2,2',4,4',6,6'-hexanitrobibenzyl, an intermediate compound used for making exanitrostilbene, is prepared by adding an aqueous alkaline metal hypochlorite solution containing an alkaline metal hydroxide to trinitrotoluene dispersed in a single solvent selected from the group consisting of methanol, ethanol, 2-methoxyethanol, isopropanol, acetone, tetrahydrofuran, N,N-dimethylformamide, N,N-dimethylacetamide, pyridine and N-methyl pyrrolidinone. The compound is then separated from the reaction mixture.

REFERENCES:
patent: 4085152 (1978-04-01), Saiter et al.

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