Process for preparing halogenated trialkyl phosphate esters

Details Process for preparing halogenated trialkyl phosphate esters Process for preparing halogenated trialkyl phosphate esters

1985-11-27

1987-12-22

Sutto, Anton H.

Organic compounds -- part of the class 532-570 series

Organic compounds

Phosphorus esters

C07F 909

Patent

active

047147717

ABSTRACT:
A method of producing a halogenated trialkyl phosphate ester which comprises admixing a halogenated hydroxy compound containing a halogen selected from the group consisting of bromine, chlorine, iodine and mixtures thereof, a phosphorus oxyhalide containing a halogen selected from the group consisting of bromine, chlorine, iodine and mixtures thereof, a solvent suitable to dissolve the halogenated hydroxy compound and the phosphorus oxyhalide, said solvent being substantially inert to hydrogen halide, and a catalyst suitable to increase the polarity of the phosphorus oxyhalide, refluxing said admixture sufficiently to form a trialkyl phosphate ester precipitate, and recovering this precipitate.

REFERENCES:
patent: 1766720 (1930-06-01), Nicolai
patent: 1840335 (1932-01-01), Horst
patent: 2624750 (1953-01-01), Pechukas
patent: 2870192 (1959-01-01), Bonstedt
patent: 3324205 (1957-06-01), Carpenter et al.
patent: 3830886 (1974-08-01), Davis et al.
patent: 4046719 (1977-09-01), Stanaback
Derwert Abstract of Japanese, 7106865.
Zakharou et al., English Language Transtation from "Aka. Nauk. SSSR, Seriyakhim", No. 11 (1971), pp. 2503-2509.
Jackson et al., "Chem. Abst.", vol. 80, (1973), 97205h.
Kosolapoff, "Organophosphorus Cpds.", 1951, pp. 211-277.

Affiliated with

Also associated with

Rating

Process for preparing halogenated trialkyl phosphate esters does not yet have a rating. At this time, there are no reviews or comments for this patent.

If you have personal experience with Process for preparing halogenated trialkyl phosphate esters, we encourage you to share that experience with our LandOfFree.com community. Your opinion is very important and Process for preparing halogenated trialkyl phosphate esters will most certainly appreciate the feedback.

Rate now

Comments { 0 }

Profile ID: LFUS-PAI-O-819454