Process for preparing ethyl .alpha.-chloroethyl carbonate

Details Process for preparing ethyl .alpha.-chloroethyl carbonate Process for preparing ethyl .alpha.-chloroethyl carbonate

1981-07-28

1983-07-19

Williams, Howard S.

Chemistry: electrical and wave energy

Processes and products

Processes of treating materials by wave energy

B01J 1912

Patent

active

043942334

ABSTRACT:
Diethylcarbonate is chlorinated with dry chlorine gas in the presence of ultraviolet rays to give ethyl .alpha.-chloroethyl carbonate in a good yield. The chlorination is preferably carried out, with or without a carbon tetrachloride solvent as a reaction medium, at a range of temperature of 45.degree. to 55.degree. C.

REFERENCES:
patent: 2918478 (1959-12-01), Newman
patent: 3454597 (1969-07-01), Tong et al.

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