Process for preparing difluorinated diazoniabicycloalkane deriva

Organic compounds -- part of the class 532-570 series – Organic compounds – Unsubstituted hydrocarbyl chain between the ring and the -c-...

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540556, 544351, C07D48708, C07B 3900

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active

053670710

ABSTRACT:
The invention is a process for preparing 1,4-diazoniabicycloalkanes of Formula I wherein the corresponding 1-hydro-4-aza-1-azoniabi-cycloalkane salt of the 1,4-diazabicycloalkane is fluorinated in the presence of an alkali metal salt under reaction conditions sufficient to form the desired 1,4-diazoniabicycloalkane. ##STR1## wherein n represents 0, 1 or 2;

REFERENCES:
patent: 2964526 (1960-12-01), Herride
patent: 4935519 (1990-06-01), Van Der Puy
patent: 5086178 (1992-02-01), Banks
Umemoto, Bull Chem Soc. Japan 64, 1081(1991).
Banks, J. Flourine Chem 55, 207(1991).
Specification of 08/163257 (1993).
Bank, J Chem Soc 1992, p. 595.

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