Process for preparing dialkylnaphthalene

Chemistry of hydrocarbon compounds – Plural serial diverse syntheses – To produce aromatic

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585313, 585449, 585467, 585475, 585481, 585320, C07C 101, C07C 264, C07C 268, C07C 522

Patent

active

060111909

ABSTRACT:
2,6-Dialkylnaphthalene is prepared from a feedstock comprising naphthalene and an alkylating agent, by a process comprising the steps:
(I) transalkylating isomers of dialkylnaphthalene and naphthalene to produce monoalkylnaphthalene and isomers of dialkylnaphthalene;
(II) separating the product obtained in step (I) into naphthalene, monoalkylnaphthalene, dialkylnaphthalene and other components;
(III) alkylating the monoalkylnaphthalene fraction from step (II) with an alkylating agent to produce dialkylnaphthalene; and
(IV) separating 2,6-dialkylnaphthalene from the dialkylnaphthalene fraction in step (II),
wherein at least step (I) or step (III) is conducted in the presence of a catalyst having a composition comprising a synthetic zeolite having an X-ray diffraction pattern with an interplanar d-spacing (.ANG.)

REFERENCES:
patent: 5001295 (1991-03-01), Angevine et al.
patent: 5292934 (1994-03-01), Sikkenga et al.
patent: 5744670 (1998-04-01), Motoyuki et al.

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