Process for preparing chain-extended organopolysiloxanes

Synthetic resins or natural rubbers -- part of the class 520 ser – Synthetic resins – From silicon reactant having at least one...

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528 12, 528 14, 528 17, 528 21, 528 23, 525477, C08G 7704

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060404124

ABSTRACT:
This specification describes and claims a process for preparing chain-extended organopolysiloxanes. The process comprises the steps of: A) mixing organopolysiloxanes having at least one silicon-bonded hydroxyl group per molecule with a polymerization catalyst to form a mixture, B) allowing the mixture of step A to react so as to produce a reaction product comprising polymerized organopolysiloxanes of which some have at least one silicon-bonded hydroxyl group per molecule and C) allowing the silicon-bonded hydroxyl group containing organopolysiloxanes of the reaction product of step B to react with a nitrogen-containing silylating agent capable of chain-extending to produce a chain-extended organopolysiloxane. Preferably the silylating agent is a cyclosilazane. Organopolysiloxanes having terminal groups other than silicon-containing hydroxyl groups and which are capable of equilibrating with the mixture of step A and/or the reaction product of step B may also be introduced prior to step C. The chain-extended organopolysiloxanes are suitable for use in sealant compositions.

REFERENCES:
patent: 3133110 (1964-05-01), Morehouse et al.
patent: 4012375 (1977-03-01), Hahn
patent: 4725643 (1988-02-01), Burkhardt
patent: 4835237 (1989-05-01), Burkhardt et al.
patent: 4902813 (1990-02-01), Wegehaupt et al.

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