Organic compounds -- part of the class 532-570 series – Organic compounds – Oxygen containing
Patent
1989-05-30
1990-05-29
Mars:, Howard
Organic compounds -- part of the class 532-570 series
Organic compounds
Oxygen containing
560236, 560264, 560266, C07C 3136, C07C 3142
Patent
active
049297759
ABSTRACT:
This invention relates to a process for preparing high purity dibromoneopentyl glycol which comprises: (a) charging a vessel with pentaerythritol, a first portion of aqueous HBr and a catalyst; (b) maintaining the liquid contents in the vessel at a temperature from 80.degree. C. to 130.degree. C. for 1 to 3 hours; (c) adding a second portion of aqueous HBr to provide a total HBr to pentaerythritol molar ratio of 1:3 to 1:6; (d) after the foregoing aqueous HBr addition, raising the temperature of the liquid content of the vessel to 120.degree. C. to 180.degree. C.; and (e) sweeping the headspace of the vessel during at least (b), (c) and (d) with an inert gas and removing the sweep gas and any vapors formed during the process from the vessel.
REFERENCES:
patent: 3876509 (1975-04-01), Davis et al.
patent: 3883581 (1975-05-01), Davis et al.
patent: 3932541 (1976-01-01), Davis et al.
patent: 4154966 (1979-05-01), Weil
Wawzonek et al., Organic Synthesis, vol. 38 (1958), pp. 68-70.
Ethyl Corporation
Mars: Howard
Speilman, Jr. Edgar E.
LandOfFree
Process for preparing brominated pentaerythritols does not yet have a rating. At this time, there are no reviews or comments for this patent.
If you have personal experience with Process for preparing brominated pentaerythritols, we encourage you to share that experience with our LandOfFree.com community. Your opinion is very important and Process for preparing brominated pentaerythritols will most certainly appreciate the feedback.
Profile ID: LFUS-PAI-O-522305