Process for preparing alumina being suitable for layer chromatog

Coating processes – With post-treatment of coating or coating material – Heating or drying

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423625, 423630, 21098C, C01F 702, B01D 1508

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active

042256399

ABSTRACT:
The invention relates to a process for preparing alumina being suitable for layer chromatography.
The alumina suitable for layer chromatography is prepared in accordance with the invention in such a manner that an aluminium trinydroxyde containing 34 to 37% by weight of bayerite, 3 to 5% by weight of pseudoboehmite and 60 to 62% by weight of amorphous aluminium trihydroxide is heated at 300.degree. C. to 400.degree. C. for 2 to 4 hours.
The activated alumina thus produced is snow-white, has a large specific surface and its average grain size is within the range between 8 and 20 .mu.m.
The product complies with the requirements of layer chromatographical technique.

REFERENCES:
patent: 2247624 (1941-07-01), Wall
patent: 2894915 (1959-07-01), Keith
patent: 2898307 (1959-08-01), Keith
patent: 3539468 (1970-11-01), Wright
patent: 3542588 (1970-11-01), Heidbrink
patent: 3726405 (1973-04-01), Engelbrecht
Frey, H. "Chromatographic Separations on Ultrathin Silica Gel and Aluminum Oxide Layers" in Chemical Abstracts vol. 77, 1972, #96524n. _

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