Process for preparing acyloxysilanes

Organic compounds -- part of the class 532-570 series – Organic compounds – Silicon containing

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C07F 708, C07F 709

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active

053877063

ABSTRACT:
A process for the preparation of acyloxysilanes. The process comprises contacting a chlorosilane with a carboxylic acid in a film forming an equilibrium mixture of acyloxysilane and hydrogen chloride. The film is heated at a temperature sufficient to cause vaporization of the hydrogen chloride from the equilibrium mixture thereby increasing the yield of acyloxysilane in the equilibrium mixture. In a preferred process, the process is run in a falling-film type reactor or a wiped-film type reactor.

REFERENCES:
patent: 3974198 (1976-08-01), Ashby
patent: 4176130 (1979-11-01), John et al.
patent: 4329484 (1982-05-01), Petersen
patent: 4332956 (1982-06-01), Tolentizio
patent: 4379766 (1983-04-01), Mack et al.

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