Process for preparing active oxide powders

Chemistry of inorganic compounds – Rare earth compound

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Details

423592, 423608, 423636, C01F 1700, C01G 2502, C01F 502

Patent

active

041407717

ABSTRACT:
An improved process for preparing active oxide powders in which cation hydroxide gels, prepared in the conventional manner are chemically dried by alternately washing the gels with a liquid organic compound having polar characteristics and a liquid organic compound having nonpolar characteristics until the mechanical water is removed from the gel. The water-free cation hydroxide is then contacted with a final liquid organic wash to remove the previous organic wash and speed drying. The dried hydroxide treated in the conventional manner will form a highly sinterable active oxide powder.

REFERENCES:
patent: 2610104 (1954-09-01), Friedel
patent: 3254949 (1966-06-01), Clearfield
Hardy et al., "ORNL-4000", Oak Ridge National Lab., Oak Ridge, Tenn., Aug. 967, 65 pages.

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