Process for preparing acetylsulfaguanidine

Chemistry of carbon compounds – Miscellaneous organic carbon compounds – C-metal

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424321, C07C14358

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active

042105935

ABSTRACT:
A method suitable for the continuous preparation of acetylsulfaguanidine is described which comprises exposing a thin layer of a concentrated aqueous solution of ammonium acetylsulfanilylcyanamide to microwave radiation until essentially anhydrous ammonium acetylsulfanilylcyanamide is obtained in the form of a glassy, non-crystalline sheet, and converting the dry ammonium acetylsulfanilylcyanamide to acetylsulfaguanidine by heating.

REFERENCES:
patent: 2380006 (1945-07-01), Winnek et al.
patent: 2463793 (1949-03-01), Mosnier
Copson, Microwave Heating, pp. 371 to 372, The Avi Publishing Co., Inc., Conn. USA (1962).
Chem. Abstracts, vol. 55, col. 8355b (1961).

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