Chemistry of carbon compounds – Miscellaneous organic carbon compounds – C-metal
Patent
1978-05-04
1980-07-01
Randolph, John D.
Chemistry of carbon compounds
Miscellaneous organic carbon compounds
C-metal
424321, C07C14358
Patent
active
042105935
ABSTRACT:
A method suitable for the continuous preparation of acetylsulfaguanidine is described which comprises exposing a thin layer of a concentrated aqueous solution of ammonium acetylsulfanilylcyanamide to microwave radiation until essentially anhydrous ammonium acetylsulfanilylcyanamide is obtained in the form of a glassy, non-crystalline sheet, and converting the dry ammonium acetylsulfanilylcyanamide to acetylsulfaguanidine by heating.
REFERENCES:
patent: 2380006 (1945-07-01), Winnek et al.
patent: 2463793 (1949-03-01), Mosnier
Copson, Microwave Heating, pp. 371 to 372, The Avi Publishing Co., Inc., Conn. USA (1962).
Chem. Abstracts, vol. 55, col. 8355b (1961).
American Cyanamid Company
Costello, Jr. Charles F.
Randolph John D.
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