Process for preparing a sol-gel solution and use of this...

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Reexamination Certificate

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C516S099000, C516S102000, C516S104000, C516S098000, C516S109000, C427S299000, C427S372200, C427S508000, C428S336000, C428S457000

Reexamination Certificate

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08084123

ABSTRACT:
The invention relates to a process for preparing a stable sol-gel solution. The solution may be used to form coating materials for metallic substrates, such as silver-based substrates for use in mirrors. The process includes the steps of preparing a sol-gel solution by bringing one or more molecular metal and/or metalloid precursors into contact with a medium comprising an organic solvent, adding at least one mercaptoorganosilane compound to the solution, hydrolyzing the solution obtained, and then adding one or more complexing agents to the solution.

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patent: 4645712 (1987-02-01), Ishigaki et al.
patent: 5614327 (1997-03-01), Morello
patent: 6387453 (2002-05-01), Brinker et al.
patent: 6540844 (2003-04-01), Crook
patent: 2002/0010273 (2002-01-01), Matsumura et al.
patent: 2004/0131867 (2004-07-01), Bier et al.
patent: 0 818 561 (1998-01-01), None
Cai, Mei, et al. “Surface Vibrational Spectroscopy of Alkylsilane Layers Covalently Bonded to Monolayers of (3-Mercaptopropyl)trimethoxysilane on Ag Substrats”, Langmuir, 2000, pp. 3446-3453, vol. 16.

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