Process for preparing a myrcenol, cis-ocimenol mixture substanti

Details Process for preparing a myrcenol, cis-ocimenol mixture substanti Process for preparing a myrcenol, cis-ocimenol mixture substanti

1978-11-13

1981-05-05

Morgenstern, Norman

Organic compounds -- part of the class 532-570 series

Organic compounds

Oxygen containing

260459R, 2605676H, 2605676M, 260583H, 260598, 546184, 546240, 546248, C07C 2944, C07C 2988, C07C 2900, C07C 3302

Patent

active

042660874

ABSTRACT:
The instant invention provides a new and improved method of preparing the Diels Alder mixture of 3 and 4-(4-methyl-4-hydroxyamyl).DELTA..sup.3 -cyclohexenecarboxaldehyde from the readily available myrcene. The novel sequence includes a synthesis of a novel myrcenol, ocimenol intermediate which is substantially free of trans-ocimenol.

REFERENCES:
patent: 2871271 (1959-01-01), Booth
patent: 2947780 (1960-08-01), Teegarden et al.
patent: 3075003 (1963-01-01), Blumenthal
patent: 3176022 (1965-03-01), Blumenthal
patent: 3344171 (1967-09-01), Lemberg
patent: 3433839 (1969-03-01), Moroe et al.
patent: 3758590 (1973-09-01), Bledsoe et al.
patent: 3932539 (1976-01-01), Kane et al.
patent: 4007137 (1977-02-01), Sanders et al.
"Org. Reactions", Cope et al., Ed. vol. 11, pp. 322-330 (Chap. 5) John Wiley & Sons, New York, N.Y. (1964).
Takabe et al., "Bull. Soc. Chem. Jap", 46, 222-225 (1973).
Takabe et al., "Chem. Letters", pp. 1025-1026 (1977).

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