Process for preparing...

Organic compounds -- part of the class 532-570 series – Organic compounds – Amino nitrogen containing

Reexamination Certificate

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C564S304000, C564S437000, C564S443000

Reexamination Certificate

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07030276

ABSTRACT:
A process for preparing 2-[(dimethylamino)methyl]-1-(3-methoxyphenyl)cyclohexanol with high stereoselectivity and high yield by reacting 2-[(dimethylamino)methyl]-cyclohexanone in a Grignard reaction with a Grignard compound of 3-bromoanisole in a suitable solvent and in the presence of an inorganic lithium salt and an α,ω-dialkoxyalkane.

REFERENCES:
patent: 6399829 (2002-06-01), Jarvi
patent: 6469213 (2002-10-01), Schickaneder
patent: 99 03820 (1999-01-01), None
patent: 99 61405 (1999-12-01), None

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