Process for preparing 4,4,4-trichlorobutan-1-ol

Details Process for preparing 4,4,4-trichlorobutan-1-ol Process for preparing 4,4,4-trichlorobutan-1-ol

1997-07-08

1999-02-23

Shippen, Michael L.

Organic compounds -- part of the class 532-570 series

Organic compounds

Oxygen containing

568841, C07C 2900

Patent

active

058746501

ABSTRACT:
A process for the preparation of 4,4,4-trichlorobutan-1-ol which comprises reacting allyl alcohol with chloroform in the presence of a radical initiator. Preferably the allyl alcohol is added incrementally to the chloroform over the period of the reaction.

REFERENCES:
Ameduri and Boutevin, "Synthesis of Chlorinated Telechelic Oligomers"--Macromolecules, vol. 24:9, 1991, pp. 2475-2484.
Chen et al., "Rearrangements and Conformations of Chloroalkyl Radicals by Electron Spin Resonance"--J. American Chem. Soc., vol. 96:7, 1974, pp. 2201-2208.
Imai et al., "Ring Opening Alkylation of Cyclic Ethers with .alpha.-Halogenoalkyllithiums in the Presence of Boron Trifluoride--Dithyl Ether", J. Chem. Soc., Chem Commun., 1994, pp. 2353-2354.

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