Process for preparing 1-cyclopropylalkane-1,3-diones

Organic compounds -- part of the class 532-570 series – Organic compounds – Oxygen containing

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568314, 568388, C07C 4545

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active

055457622

ABSTRACT:
1-cyclopropylalkane-1,3-diones are prepared by reacting a cyclopropyl alkyl ketone with a carboxylic ester in the presence of an alkali metal alcoholate, at temperatures of not more than 50.degree. C. in the presence of a solvent which is free of alcohol or contains only small quantities of alcohol.

REFERENCES:
patent: 3507958 (1970-04-01), Zimmermann
patent: 4256657 (1981-03-01), Wheeler
patent: 5015777 (1991-05-01), Chisolm et al.
patent: 5118681 (1992-06-01), Amick et al.
patent: 5344992 (1994-09-01), Drewes et al.
Journal of Organic Chemistry, vol. 17, pp. 685-688, 1952, George W. Cannon, et al., "Actylation Studies. I. Methyl Cycloppropyl Ketone".

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