Process for preparing 1,4:3,6-dianhydro-D-glucitol 2-nitrate

Details Process for preparing 1,4:3,6-dianhydro-D-glucitol 2-nitrate Process for preparing 1,4:3,6-dianhydro-D-glucitol 2-nitrate

1977-02-24

1977-12-27

Sebastian, Leland A.

Chemistry of carbon compounds

Miscellaneous organic carbon compounds

C-metal

424298, C07C 7702

Patent

active

040654885

ABSTRACT:
The following process for preparing 1,4:3,6-dianhydro-D-glucitol 2-nitrate is described: acylating 1,4:3,6-dianhydro-D-glucitol with 0.5 to 1.5 molar equivalents of acetic anhydride in the presence of an acid catalyst, nitrating the product so obtained with a mixture of nitric acid and acetic anhydride, hydrolyzing the product so obtained in the presence of an inorganic base and isolating 1,4:3,6-dianhydro-D-glucitol 2-nitrate. The 1,4:3,6-dianhydro-D-glucitol 2-nitrate is useful as a coronary vasodilator.

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