Process for preparing 1,1-dimethyl hydrazine

Details Process for preparing 1,1-dimethyl hydrazine Process for preparing 1,1-dimethyl hydrazine

1975-09-29

1977-09-06

Wyman, Daniel E.

Chemistry of carbon compounds

Miscellaneous organic carbon compounds

C-metal

260583N, C07C10902

Patent

active

040468127

ABSTRACT:
Unsymmetrical dimethyl hydrazine is prepared by a process wherein aqueous 1,1-dimethylurea is initially reacted with a hypochlorite salt whereupon the resultant intermediate essentially in form of a N-chloro derivative of said urea is rearranged in accordance with the Hofmann reaction to yield the desired substituted hydrazine.

REFERENCES:
patent: 2917545 (1959-12-01), Lum et al.
Adams et al., "Organic Reactions," vol. III, pp. 280-282 (1956).

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