Process for preparation of samples for analysis

Chemistry: analytical and immunological testing – Including sample preparation – Dilution

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Details

436 43, 436180, 436174, G01N 128

Patent

active

049006835

ABSTRACT:
An automated sample preparation system for chemical assay of samples of materials. The sample preparation system includes a sample preparation chamber which includes a removable cup for taking solid or very viscous samples to the sample preparation system. The cup may be attached in sealing relationship to a cap through which extends various utilities such as a mixer/grinder to grind solid samples and mix non-homogeneous samples, a fill pipe to pump in liquid samples, an effluent pipe in the sump of the cup to allow pumping of samples and solvents and a nozzle to allow liquids to be sprayed against the walls. A sample metering valve associated with the sample preparation chamber allows a known volume of sample to be isolated so that solvent may be pumped in to dilute the sample to a user defined concentration. A reversible pump is coupled by a pair of manifolds which are themselves coupled by solenoid operated valves to various sources of solvents, pressurized gas, vacuum, water, the sample preparation chamber and the assay system. A control system coordinates the operation of all remotely controllable units in the system to allow the user to customize various sample preparation processes.

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An Apparatus for Sample Preparation in a Measurement and/or Control System and the Application of this Apparatus, Priority: Swiss, 29 Aug. 1986, Ciba-Geigy AG, Case 7-16068/CIT 29 pages.

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