Process for preparation of reduced metal titanium complexes

Details Process for preparation of reduced metal titanium complexes Process for preparation of reduced metal titanium complexes

1995-04-25

1997-04-01

Nazario-Gonzalez, Porfirio

Organic compounds -- part of the class 532-570 series

Organic compounds

Heavy metal containing

556 12, 556 20, 556 52, 556 53, 556 54, 556 56, 526943, 502155, 502158, C07F 1700, C07F 700, C07F 902

Patent

active

056167482

ABSTRACT:
A process for preparing titanium or zirconium hydrocarbyloxide complexes in a reduced oxidation state comprising contacting the corresponding complex in an elevated oxidation state with lithium alkyl reducing agent and recovering the resulting product.

REFERENCES:
patent: 5264590 (1993-11-01), Strickler
J. Skupinska and W. Skupinski: "ESR Investigation of Ti.sup.+3 Compounds Supported on Inorganic Gels", React. Kinet. Catal. Lett., vol. 16, No. 2-3, 297-300; (1981).
Chemical Abstracts, vol. 95, No. 14, 5 Oct. 1981, Columbus, Ohio, Abstract No. 121521r, Skupinska, J. et al. "ESR Investigation of Titanium (+3) Compounds Supported on Inorganic Gels", p. 400.
J. Am. Chem. Soc., 3,581 (1961).
Gmelin Handbuch der Anorganischen Chemie, Springer-Verlag, p. 134, (1977).

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