Process for preparation of polyhedral oligomeric silsesquioxanes

Synthetic resins or natural rubbers -- part of the class 520 ser – Synthetic resins – From heavy metal or aluminum reactant having at least one...

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556450, 556455, 556460, 528 37, 528 40, 528 15, 528 31, 528 32, 525474, 526249, C08G 7706

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054848679

ABSTRACT:
A process for preparation of reactive polyhedral oligomeric silsesquioxanes and the subsequent synthesis of polysilsesquioxanes which produce high yield, tractable polymers containing silsesquioxane segments is provided. A trifunctional polyhedral oligomeric silsesquioxane of the formula Si.sub.7 R.sub.7 O.sub.9 (OA).sub.3 is corner capped by reacting it with a compound of the formula M-Z to form a polyhedral oligomeric silsesquioxane which can be reacted in various ways with oligomers, polymers, catalysts, or co-monomers to form polyhedral silsesquioxane polymers containing silsesquioxanes as pendant, block, or end group segments. The resulting polymers are essentially free of impurities and have controllable properties through the proper selection of the synthesis process and starting materials.

REFERENCES:
patent: 2465188 (1949-03-01), Barry et al.
patent: 3294737 (1966-12-01), Krantz
patent: 4349609 (1982-09-01), Takeda et al.
patent: 4513132 (1985-04-01), Shoji et al.
patent: 4745169 (1988-05-01), Sugiyama et al.
patent: 4871616 (1989-10-01), Kimura et al.
patent: 5039771 (1991-08-01), Morimoto et al.
patent: 5043789 (1991-08-01), Linde et al.
patent: 5047472 (1991-09-01), Weidner et al.
patent: 5047492 (1991-09-01), Weidner et al.
Feher, et al. "Silsesquioxames as Models for Silica Surfaces" J. Am. Chemical Soc. 1989, 111, pp. 1741-1748.
Schildknecht, "Vinyl and Related Polymers" 1952. p. 515.
Laine et al, Chem. Mat., (1990), V. 2:464-472.
Rahn et al, Mat. Res. Soc. Symp. Proc. (1990), V. 171:31-37.
Lichtenhan et al, "Silsesquioxane-Siloxane Copolymers from Polyhedral Silsesquioxanes," Macromolecules, 1993, 26 No. 8.
"Ladder and Spiro Polymers," Concise Encyclopedia of Polymer Sci. & Eng., 1990, pp. 516-521.
Feher et al, "Enhanced Silylation Reactivity of a Model for Silica Surfaces," J. Am. Chem Soc., 1990, 112, pp. 1931-1936.
Taylor et al, "The Preparation, Characteristics, and Use of Siloxanes as Precursors to Silicon Carbide," Polymer Preprints, vol. 32, 1991, pp. 586-587.

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