Process for preparation of non-hazardous brominating agent

Chemistry of inorganic compounds – Halogen or compound thereof – Ternary compound

Reexamination Certificate

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C423S472000, C423S499100, C252S182160, C252S187200

Reexamination Certificate

active

07459139

ABSTRACT:
A cost-effective process is described for the preparation of a stable and non-hazardous brominating reagent containing 2:1 stoichiometric ratio of alkali bromide to alkali bromate. The process comprises of reacting alkaline bromine intermediate mixture, obtained from bromine recovery plant, with chlorine gas in the presence of a strong alkali to oxidize the bromide ions to bromate ions. This brominating reagent is useful for the bromination of aromatic compounds by substitutions.

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patent: 4719096 (1988-01-01), Lesher et al.
patent: 6143698 (2000-11-01), Murphey et al.
patent: 6165343 (2000-12-01), Blum et al.
patent: 6365786 (2002-04-01), Ramachandraiah et al.
patent: 2003/0136941 (2003-07-01), Vohra et al.
patent: 84830 (1995-01-01), None
patent: 02 057207 (2002-07-01), None
English Abstract of IL 84830 dated Jan. 24, 1995 Database WPI Section CH, Week 199517 Derwent Publications (XP 002268 916).

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