Chemistry of carbon compounds – Miscellaneous organic carbon compounds – C-metal
Patent
1974-09-13
1976-08-03
Horwitz, D.
Chemistry of carbon compounds
Miscellaneous organic carbon compounds
C-metal
C07C 120
Patent
active
039729559
ABSTRACT:
In the preparation of isoprene by reacting isobutene with formaldehyde to produce 4,4-dimethyl-m-dioxane in a first stage, and decomposing the dioxane to isoprene and formaldehyde in a second stage, formaldehyde in the effluent streams of either or both of said stages is recovered. The formaldehyde-containing liquids are distilled to separate high boilers; the overhead, which is formaldehyde-rich, is extracted with isobutene feed to the process, whereby the isobutene extracts low boilers from the formaldehyde-containing liquid; and the formaldehyde-containing liquid, having at some point after said distillation been treated with an alkaline material, is subjected to rectification to produce as head product, the recovered formaldehyde.
REFERENCES:
patent: 3057923 (1962-10-01), Hellin et al.
patent: 3773847 (1973-11-01), Losacker et al.
Halcour Kurt
Losacker Paul
Schwerdtel Wulf
Swodenk Wolfgang
Bayer Aktiengesellschaft
Horwitz D.
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