Process for preparation of isocyanate compounds

Organic compounds -- part of the class 532-570 series – Organic compounds – Isocyanate esters

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560 24, 560157, 560158, C07C26300, C07C26100

Patent

active

059144289

ABSTRACT:
An aliphatic diisocyanate compound is prepared in a high yield by reacting dimethyl carbonate with an aliphatic diamine in the presence of an alkali catalyst to produce a corresponding urethane compound; and, within 48 hours after the completion of the preparation of the urethane compound, thermally decomposing the urethane compound under a reduced pressure of 1 to 700 Torr in a high-boiling-point solvent.

REFERENCES:
patent: 3919279 (1975-11-01), Rosenthal et al.
patent: 4081472 (1978-03-01), Tsumura et al.
patent: 4330479 (1982-05-01), Merger et al.
patent: 4395565 (1983-07-01), Romano et al.

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